As a teenager with an interest in chemistry and living in the country with a barn suitably far from the house to dampen the sound of what I was doing...I started making gunpowder in small quantities - about 250g at a time. I was very careful, took care to use wooden instruments to prevent sparks and carefully produced about 1 kg of very fine powder.
Produced a very large rocket over 1 meter long, suitably filled it with powder, carefully fused it so I had an escape period when ignition started and tested in the local fields when my parents were out.
It appears I made a fundamental error as the powder had not been packed firmly enough so when the fuse lit the gunpowder, instead of the rocket burning and rising into the air, all the powder ignited all at once. I was about 50 meters away, crouching down behind a friendly tree stump so was not hurt..BUT:
I was deafened for several hours after the explosion and the sound was heard a mile away in the nearby town.
I hastily mended the hole in the field, removed all evidence of a rocket - not much was left - and kept quiet. The local paper reported "a mysterious explosion" blamed on a naval plane from nearby Lossiemouth breaking the sound barrier.
I gave up chemistry after that and concentrated on physics....